Nuclear Magnetic Resonance Spectroscopy Lab: 4 Resources found

1. The JEOL 400 MHz NMR features a 5mm Broad Band Probe. 2. It can observe 1H, 13C, 11B, 19F, 29Si, and 31P nuclei in solution. 3. 24 Carousel Autosampler. 4. Automatic Tuning and Matching 5. Delta 5.3 software used for data acquisition and processing, as well as MNova software that can be used for processing. 6. It can perform Variable Temperature Experiments from -100°C to 150°C. 7. The JEOL can perform 2D COSY, HSQC, HMBC, HMQC, NOESY, ROESY, and 1H-15N HMBC. It can run presaturation and water suppression. 8. USERS NEED TO SUPPLY THEIR OWN 5mm NMR TUBES AND DEUTERATED SOLVENTS All new users can contact Wendy Gavin to discuss training at wendy_gavin@uml.edu. Additional pricing for academic and government groups is available upon request.

ADVANCED NMR Includes ¹³C NMR and 2D NMR experiments, including COSY, HSQC, and HMBC, using standard acquisition parameters. Price includes an NMR tube and deuterated solvent (CDCl₃, D₂O, or DMSO-d₆). Samples must contain a minimum of 25 mg of material for acquisition using the standard/default number of scans. Additional Acquisition Time The per-sample rates are based on standard acquisition parameters and the minimum recommended sample quantities listed above. Samples requiring additional scans, longer acquisition times, specialized parameters, or additional NMR experiments can be accommodated and will be charged at an additional rate. Data Delivery Raw NMR data will be provided to the customer. Data processing, spectral interpretation, and compound identification are not included in the standard per-sample price.

STANDARD 1D NMR Includes ¹H (proton), ¹⁹F, or ³¹P NMR spectroscopy using standard acquisition parameters. Price includes an NMR tube and deuterated solvent (CDCl₃, D₂O, or DMSO-d₆). Samples must contain a minimum of 5 mg of material for acquisition using the standard/default number of scans. Additional Acquisition Time The per-sample rates are based on standard acquisition parameters and the minimum recommended sample quantities listed above. Samples requiring additional scans, longer acquisition times, specialized parameters, or additional NMR experiments can be accommodated and will be charged at an additional rate. Data Delivery: Raw NMR data will be provided to the customer. Data processing, spectral interpretation, and compound identification are not included in the standard per-sample price.